Sample | Yield | Elemental analysis | Thermogravimetry | FTIR Relative peak intensity ratios | |||||||||||
---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
C | H | N | O | H/C | N/C | O/C | Humidity | 1st onset | Ash | Aliph./Arom. | Arom./O– groups | Arom./Amid. | |||
[wt%] | [at%] | [at%] | [at%] | [at%] | [1] | [1] | [1] | [wt%] | [°C] | [wt%] | [1] | [1] | [1] | ||
HA | 10.7 | 43.5 | 37.0 | 0.9 | 18.6 | 0.85 | 0.02 | 0.43 | 5.8 | 202.8 | 0.9 | 1.24 | 0.93 | 1.08 | |
RHA samples | 10 N | 11.0 | 40.0 | 45.8 | 0.6 | 13.6 | 1.15 | 0.02 | 0.34 | 5.4 | 226.6 | 0.5 | 1.23 | 0.99 | 1.08 |
20 N | 28.4 | 38.2 | 42.7 | 2.1 | 16.9 | 1.12 | 0.06 | 0.44 | 5.8 | 134.8 | 0.3 | 1.20 | 0.96 | 0.98 | |
30 N | 24.6 | 37.9 | 42.0 | 2.4 | 17.7 | 1.11 | 0.06 | 0.47 | 5.8 | 162.4 | 0.4 | 1.24 | 0.96 | 0.95 | |
40 N | 18.8 | 38.3 | 40.9 | 2.9 | 17.8 | 1.07 | 0.08 | 0.46 | 4.3 | 153.1 | 0.4 | 1.13 | 0.97 | 0.94 | |
50 N | 34.7 | 38.4 | 41.1 | 2.7 | 17.8 | 1.07 | 0.07 | 0.46 | 4.9 | 152.6 | 0.5 | 1.20 | 0.97 | 0.93 | |
65 N | 35.5 | 36.7 | 43.5 | 2.9 | 17.0 | 1.19 | 0.08 | 0.46 | 5.2 | 169.7 | 0.5 | 1.18 | 0.98 | 0.90 | |
5P | 10.1 | 41.6 | 43.4 | 0.9 | 14.1 | 1.04 | 0.02 | 0.34 | 6.2 | 200.1 | 0.3 | 1.22 | 0.98 | 1.18 | |
10P | 9.1 | 40.2 | 44.5 | 0.8 | 14.5 | 1.11 | 0.02 | 0.36 | 6.2 | 192.2 | 0.3 | 1.25 | 0.98 | 1.12 | |
20P | 13.6 | 39.2 | 45.1 | 0.7 | 15.0 | 1.15 | 0.02 | 0.38 | 4.7 | 169.8 | 0.3 | 1.31 | 0.98 | 1.14 | |
30P | 7.0 | 38.9 | 46.6 | 0.4 | 14.1 | 1.20 | 0.01 | 0.36 | 3.7 | 204.0 | 0.3 | 1.24 | 0.99 | 1.07 |