Table 1 D-optimal design arrangement and responses for HYOOA
From: Synthesis and optimization ring opening of monoepoxide linoleic acid using p-toluenesulfonic acid
Run | Coded independent variable levels | Responses | |||||
|---|---|---|---|---|---|---|---|
No. | OAa/MEOAbPTSAc/MEOA | Temp. | Time | OOCd | Yield | IV | |
(mol/mol, X1) | (mol/mol, X2) | (°C, X3) | (h, X4) | (%, Y1) | (%, Y2) | (mg/g, Y3) | |
Run | Coded independent variable levels | Responses | |||||
1 | 0.20 | 0.90 | 90 | 4.50 | 2.60 | 70.5 | 101.4 |
2 | 0.20 | 0.40 | 90 | 3.00 | 0.90 | 82.1 | 114.3 |
3 | 0.40 | 0.65 | 90 | 4.50 | 3.80 | 61.1 | 84.2 |
4 | 0.40 | 0.65 | 100 | 6.00 | 3.20 | 56.4 | 91.9 |
5 | 0.40 | 0.40 | 100 | 4.50 | 3.40 | 84.5 | 90.3 |
6 | 0.30 | 0.78 | 100 | 3.75 | 3.10 | 70.4 | 94.1 |
7 | 0.60 | 0.40 | 110 | 6.00 | 2.70 | 58.3 | 100.2 |
8 | 0.60 | 0.40 | 110 | 3.00 | 2.40 | 55.5 | 109.7 |
9 | 0.60 | 0.90 | 90 | 6.00 | 2.10 | 27.8 | 110.8 |
10 | 0.60 | 0.90 | 90 | 3.00 | 1.80 | 35.7 | 112.3 |
11 | 0.20 | 0.40 | 100 | 6.00 | 1.50 | 81.5 | 112.5 |
12 | 0.60 | 0.90 | 90 | 3.00 | 2.90 | 55.6 | 99.8 |
13 | 0.20 | 0.90 | 110 | 6.00 | 3.05 | 70.9 | 88.5 |
14 | 0.60 | 0.40 | 90 | 4.50 | 3.50 | 65.9 | 88.9 |
15 | 0.60 | 0.65 | 100 | 4.50 | 0.60 | 74.3 | 122.2 |
16 | 0.60 | 0.90 | 90 | 6.00 | 0.80 | 53.7 | 120.4 |
17 | 0.60 | 0.90 | 110 | 4.50 | 0.40 | 50.8 | 123.9 |
18 | 0.20 | 0.40 | 90 | 3.00 | 0.30 | 80.1 | 125.2 |
19 | 0.40 | 0.40 | 90 | 6.00 | 2.95 | 65.1 | 94.1 |
20 | 0.60 | 0.40 | 110 | 3.00 | 1.40 | 58.4 | 114.1 |
21 | 0.20 | 0.90 | 110 | 3.00 | 0.20 | 79.5 | 127.4 |
22 | 0.40 | 0.65 | 110 | 4.50 | 0.90 | 80.1 | 118.7 |
23 | 0.60 | 0.40 | 110 | 6.00 | 0.70 | 40.8 | 121.1 |
24 | 0.20 | 0.40 | 110 | 4.50 | 0.05 | 84.6 | 134.8 |
25 | 0.20 | 0.65 | 90 | 6.00 | 0.60 | 82.4 | 122.5 |